The quantitative distribution of As, Cu, Pb, Zn elements in water and soils around Giáp Lai and Minh Quang sulfur deposits is presented in this work. The preliminary results delineate the following: i) The content of As in water is quite low and is below the polluted limit. The soils was symptomatic of pollution by As at low level. ii) The contents of Cu and Zn are higher than that of Pb, especially in some localities, Cu and Zn contents are over the permissible threshold of the surface water quality and form high anomalies