Liquid waste from Nong Son uranium ore processing is treated with concentrated acid, agglomerated, leached, run through ion exchange and then treated with H2O2 to precipitate yellowcake. The liquid radioactive waste has a pH of and a high content of radioactive elements, such as: [U] = ppm and [Th] = ppm. In addition, this waste contains many polluted chemical elements with high content, such as arsenic, mercury, aluminum, iron, zinc, magnesium, manganese and nickel. The application of the triditional method as one stage.