The development of concept in structural morphology lets description the location of nickel nanoclusters in conductive organic polymers, which may be a new kind of structure in conductive organic polymer composites family. As a new route, such the development was supported by electrochemical two-pot process, on which polianiline containing nanoclusters of nickel incorporated in layer by layer were prepared, in H2SO4 M solutions. The presence of nickel nanoclusters in polymer matrix and the changes in morphology were confirmed by SEM/EDS
