The electrophoretic deposition (EPD) method was adopted for a fabrication of nanocomposite layers composed of ZnO particles covered by the polythiopene shell in a reduced state. This composite was prepared by oxidative polymerization of thiophene monomer with iron (III) chloride as a catalyst in the presence of ZnO particles. After polymerization, polythiophene in oxidized form was reduced by the extraction in methanol. Electrochemical properties of the obtained composite were measured by cyclic voltammetry and electrochemical impedance spectroscopy. The semiconductive behavior was studied UV photoelectrochemical measurements.
