The first lab session is dedicated to the characterization of the 5,10,15,20-tetraphenylporphyrin (TPP) as well as the synthesis of the corresponding Fe(II), Co(II), Ni(II), Cu(II) and Zn(II) complexes. The second session involves the spectroscopic characterization (UV-vis, 1H-NMR, and IR) of the prepared metalloprophyrins. The students relate the experimental results with the provided theoretical data based on quantum chemical calculations. | An undergraduate experiment using microwave-Assisted synthesis of first Raw metalloporphyrins: Characterizations and spectroscopic study
