Catalyst TiO2 with N-doped, Mg-doped and N-Mg co-doped were created by impregnation method with Mg(NO3)2 (add Mg in) and mix method with urea (add N in). The XRD, SEM, DR, BET, FT-IR measurements were carried out for structural characterization of the TiO2 samples. The result performed, compared with the sample of initial TiO2-P25 particle size and specific surface area, samples of doped-catalyst changed insignificantly. | Enhance the activity of the photocatalyst TiO2-P25 degussa by doping it with N and Mg on degradation of phenol under visible light