In this study, we present some results on the structure and properties of the solid solution of – BiFeCoO3 (BKT – BFCO) by Sol-gel method. Crystal structures of BKT – BFCO solid solutions were studies by XRD and Raman spectroscopy. The results were in good agreement with the previous reports of – BiFeO3 (BKT – BFO) and – BiCoO3 (BKT – BCO) solid solutions. | Fabrication and properties of Co doped – BiFeO3 solid solution