A magnetic Fe3O4 @ montmorillonite composite was prepared and used for the separation of lead and cadmium from aqueous solutions. For this purpose, magnetite (Fe3O4) was generated by co-precipitation of FeSO4 and FeCl3 onto montmorillonite. The effects of various experimental parameters such as pH of the solution, amount of sorbent, initial concentration of analytes, and contact time on the sorption efficiencies of lead and cadmium ions were investigated and optimized by applying a batch technique. The concentrations of analytes were determined by high resolution continuum source flame atomic absorption spectrometry. |